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911.
采用二元混合自组装膜修饰纳米金颗粒,在经自组装单分子层修饰的金电极上阵列式排布,并通过共价键固定抗体形成生物敏感膜.采用原子力显微镜、扫描电镜和阻抗谱分别对电极表面的修饰过程进行了表征.纳米粒子在微电极表面均匀分布,没有明显的团聚,并且可实现抗体有效固定.基于标准互补金属氧化物半导体(Complementary met...  相似文献   
912.
李洋  孙楫舟  边超  佟建华  夏善红 《分析化学》2011,(11):1621-1628
基于循环伏安扫描(CV)的电化学沉积方法制备出多孔性纳米簇状结构铜膜,结合采用微机电系统(Micro electro mechanical systems,MEMS)技术制备的微电极芯片,研制出用于NO3-检测的安培型微传感器。考察该微传感器对NO3-的响应性能,在6.25~300mmol/L浓度范围内,灵敏度为0.0526mA/(mmol/L),线性度99.93%;在300~3500mmol/L浓度范围内,灵敏度为0.0353mA/(mmol/L),线性度99.18%。与文献报道相比,该传感器表现出更高的灵敏度。考察水体中常见的NO2-,Cl-,HPO42-/PO43-,SO42-,HCO3-/CO23-,Na+和K+等离子对该传感器的干扰性能,传感器表现出较好的抗干扰性能。采用该微传感器对实际水样进行测试,测试结果与具有权威资质的测试公司的测试结果之间具有一定的相关性。实验结果表明,采用循环伏安沉积方法在微电极表面制备的纳米簇状结构的铜敏感膜,比表面积大,催化活性高,对NO3-表现出了很好的敏感特性和选择性,适用于对微量NO3-的检测。  相似文献   
913.
基于DDE接口技术的计算机辅助装调方法   总被引:1,自引:0,他引:1  
刘志祥  马冬梅  田园  卞江 《应用光学》2009,30(3):486-490
根据波前拟合和计算机辅助装调的算法原理,基于动态数据交换(DDE)接口技术和泽尼克多项式拟合技术,采用阻尼最小二乘法,运用MATLAB和ZEMAX联合计算实现了计算机辅助装调。利用DDE接口在ZEMAX和MATLAB之间进行通讯,并用MATLAB编写了能够生成各阶泽尼克圆多项式和环多项式的基底矩阵函数的可视化的计算机辅助装调程序,实现了程序的通用性及易用性。使用该程序对大遮拦比光学系统进行模拟装调,验证了程序的正确性。为了确认泽尼克圆多项式在环域上的相关性对计算机辅助装调结果的影响,分别采用泽尼克圆多项式和环多项式进行模拟装调。模拟结果表明:计算机辅助装调使用这两种泽尼克多项式均可行。  相似文献   
914.
The reconstruction algorithm for BESⅢ Muon Counter, MucRecAlg, is developed with the object-oriented language C++ in BESⅢ offline software environment. MucRecAlg consists of the following functions: to find track seeds either from extrapolation of tracks in the main drift chamber or from the fired strips in muon counter, to select fired strips associated to the candidate tracks, to fit the candidate tracks with a linear or quadratic function and to calculate other parameters of the tracks for muon identification. Monte Carlo samples are generated to check the performance of the reconstruction package, such as reconstruction efficiency, muon remaining rate and pion rejection rate, etc. The preliminary results show that the pion rejection rate is around 3%-4% while the muon remaining rate is better than 90% in 0.4-1.6 GeV/c momentum region, which meets the requirement as shown in the design report.  相似文献   
915.
Diagnosis of methane plasma, generated in an atmospheric pressure dielectric barrier discharge (DBD) microplasma jet with a quartz tube as dielectric material by a 25 kHz sinusoidal ac power source, is conducted by optical emission spectroscopy (OES). The reactive radicals in methane plasma such as CH, C2, and Ha are detected insitu by OES. The possible dissociation mechanism of methane in diluted Ar plasma is deduced from spectra. In addition, the density of CH radical, which is considered as one of the precursors in diamond-like (DLC) film formation, affected by the parameters of input voltage and the feed gas flow rate, is emphasized. With the Boltzmann plots, four Ar atomic spectral lines (located at 675.28nm, 687.13nm, 738.40nm and 794.82nm, respectively) are chosen to calculate the electron temperature, and the dependence of electron temperature on discharge parameters is also investigated.  相似文献   
916.
With a 15M J/ψ inclusive Monte Carlo sample, the absolute branching fraction of J/ψ→γ\η' from the J/ψ inclusive photon spectrum is measured to be Br(J/ψ→γ\η')=(4.68±0.08±0.27)×10-3, which is in good agreement with the input value. The J/ψ→γfJ(2220) is also searched for using the same sample. Under our assumptions, the statistical significances of J/ψ→γfJ(2220) are larger than 7\σ.  相似文献   
917.
A novel integratable and high speed InGaAsP multi-quantum well (MQW) complex-coupled distributed feedback (DFB) laser is successfully fabricated on a semi-insulating substrate. The fabricated ridge DFB laser exhibits a threshold current of 26 mA, a slope efficiency of 0. 14 W·A^-1 and a side mode suppression ratio of 40 dB together with a 3 dB bandwidth of more than 8 GHz. The device is suitable for 10 Gbit/s optical fiber communication.  相似文献   
918.
溶液氢离子浓度计算涉及大量公式及繁杂的使用条件,是公认的教学重点和学习难点。将分布分数代入质子条件式即得关于氢离子浓度的一元高次方程,可用MATLAB方便地求解。因此,只要会写质子条件式就能迅速得到氢离子浓度,从而摆脱大量公式的烦扰,便于学生将精力更有效地集中于分析化学主体知识的学习。  相似文献   
919.
A robust time-dependent approach to the high-resolution photoabsorption spectrum of Rydberg atoms in magnetic fields is presented. Traditionally we have to numerically diagonalize a huge matrix to solve the eigen-problem and then to obtain the spectral information. This matrix operation requires high-speed computers with large memories. Alternatively we present a unitary but very easily parallelized time-evolution method in an inexpensive way, which is very accurate and stable even in long-time scaie evolution. With this method, we perform the spectral caiculation of hydrogen atom in magnetic field, which agrees well with the experimentai observation. It can be extended to study the dynamics of Rydberg atoms in more complicated cases such as in combined electric and magnetic fields.  相似文献   
920.
The N-Ag codoped ZnO films are deposited on quartz glass substrates by ultrasonic spray pyrolysis technology. The results indicate that the p-type conductivity in ZnO films is greatly enhanced by the double acceptor codoping of N and Ag compared with that of Ag- and N-monodoped ZnO films, and the NAg codoped low-resistivity p-type ZnO films with the resistivity of 1.05 Ω·cm, relatively high carrier concentration of 5.43×10^17 cm^-3, and Hall mobility of 10.09 cm^2 V^-1s^-1 are obtained under optimized conditions. This achievement confirms that p- type ZnO with acceptable properties for optoelectronic applications could be realized by simultaneous codoping with two potential acceptors.  相似文献   
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